Structure
| TCI Product No. : | T1874 | |||||||||
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| Stock Status : |
Status at 03:00 a.m. on Feb 09, 2012 (IST) * Items available from stock in Japan will be delivered in 7 business days |
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| Purity / Analysis Method : | >97.0%(GC)(T) | |||||||||
| Storage : | Refrigerator | |||||||||
| M.F. / M.W. : | C8H20N4=172.28 | |||||||||
| CAS Number : | 294-90-6 | |||||||||
| Related CAS Number : | ||||||||||
| MDL Number : |
| mp : | 111 °C |
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Cyclen-catalyzed Henry reaction (nitroaldol reaction) Typical procedure: Nitromethane (122 mg) is added to the solution of benzaldehyde (106 mg) in THF (1 mL). Then, cyclen (8.6 mg) is added. The solution is stirred at room temperature for 24 h. Volatile components are removed under reduced pressure and the residue is purified by chromatography on silica gel (eluent: pentane/diethyl ether) to give 2-nitro-1-phenylethanol (134 mg, 80 %). |
| Beilstein : | 26(5)11,23 |
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| RTECS# : | XA5253000 |
| TCI Product Literature : | |
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| Related Categories : |
Functional Materials
Macrocycles for Host-Guest Chemistry
Crown Ethers
Biochemistry Polyamines Polyamines Cyclic Polyamines |